How a Muffle Furnace Works / Types of Muffle Furnaces.

By Miriam Carrillo, 14 October 2024

Muffle furnaces are indispensable tools across various scientific and industrial fields, providing precise and controlled high-temperature environments for a wide range of applications. Whether you are ashing samples, heat-treating materials, or conducting complex thermal analyses, a muffle furnace is a reliable partner that ensures your results are both accurate and repeatable.

A muffle furnace consists of a heating element enclosed within a refractory-lined chamber, known as the muffle. The refractory material provides insulation and ensures uniform heating, preventing direct contact between the samples and the heating elements. Muffle furnaces are designed for rapid heating, temperature recovery, and cooling, all within self-contained, energy-efficient cabinets. They separate the object being heated from the byproducts of combustion, ensuring a clean environment.

Laboratory chamber furnaces are available with a range of maximum temperatures, which depend on the type of heating elements used in their construction. The most common have metallic wire heating elements with maximum temperatures ranging from 1000°C to 1200°C. Laboratory furnaces with silicon carbide heating elements can reach 1600°C, while those with molybdenum disilicide heating elements can achieve temperatures of up to 1800°C, making them suitable for the most demanding industrial processes. This high-temperature capability ensures consistent performance and reliability in extreme conditions.

Choosing the right furnace is essential for achieving optimal results and ensuring the purity and quality of your samples. Understanding the functions and applications of each type of furnace will guide you in selecting the best option for your needs. Let’s explore the different types of furnaces available on the market.

Types of laboratory furnaces:

  • Box Laboratory Furnace

A box furnace is a versatile piece of equipment used for high-temperature applications. Box furnaces use swing out doors or vertical lifts to allow products in a range of sizes to be put inside the furnace. Commonly used in chemistry, materials science, and engineering. These furnaces have a wide temperature range and can heat materials up to 1800°C.

The outer structure, the heating chamber, and the heating elements with temperature control systems are their three main components. The exterior is made of durable, heat-resistant materials such as steel, ensuring longevity and safety. The heating elements, usually made from materials like Kanthal or silicon carbide, surround the muffle and generate the required heat. These furnaces come in various sizes and shapes and can hold several different samples at once.

Muffle furnaces are a subclass of box furnaces, they are compact countertop heating sources with insulated fire brick walls to maintain high temperatures. They allow rapid high-temperature heating, recovery, and cooling in self-contained, energy-efficient cabinets. This is ideal for ashing samples, heat treating applications, and materials research

Muffle laboratory furnace can heat up to 1200°C and can handle a variety of materials like ceramics, glass, metals, and plastics.

Across International Ai 1050 Compact Muffle Furnace

  • Tube Laboratory Furnace

The exterior of a tube furnace is built from strong, heat-resistant materials, providing the durability needed to withstand high-temperature demands. At its core is the cylindrical tube, which holds the material being heated. This tube is made from ceramics or other heat-resistant materials. Surrounding the cylindrical tube are the heating elements, strategically positioned to ensure consistent temperature distribution throughout the furnace. The design facilitates precise control over the temperature along the length of the tube, which is the area within the furnace where the temperature is most consistent. 

They can reach temperatures of up to 1800°C and enable rapid heat up, recovery, and cool down. The samples are inserted into the central part of the furnace tube, where they undergo heating. Tube furnaces are ideal for processing smaller samples due to their limited volume capacity and rapid heat-up times. Additionally, they also allow for a controlled atmosphere around the samples, which helps preserve purity and prevent contamination.

There are three types of tube furnaces available, each tailored to meet a wide range of industrial needs and specifically designed for certain applications.

A vertical tube furnace is often employed in applications that require precise control over heating and cooling rates, such as material testing, thermal processing, and chemical reactions. Its design is advantageous for processes where samples need to be introduced from the top, making it ideal for specific chemical and physical experiments. The vertical configuration also offers a space saving solution, making it perfect for laboratories with limited room. Moreover, the vertical setup can be beneficial in processes where gravity assists with even heat and material distribution, enhancing the efficiency of the experiment or production process.

The horizontal tube furnace provides consistent heating across the entire tube length and can accommodate various tube sizes. The horizontal design also allows for easy placement and removal of samples, making it especially useful for experiments that require manipulation or observation during heating.

A rotary tube furnace features a rotating mechanism that allows the tube to rotate during operation. This rotation promotes more even heat distribution, prevents the settling of samples, and enhances the efficiency of heat transfer leading to faster processing times and more uniform results. These furnaces are well suited for continuous processing and are capable of handling both small and large sample volumes.  They are especially valuable in applications like powder metallurgy, material blending, and chemical reactions, where consistent heating and continuous mixing are essential. They are also widely used in industries that process granular or powdery materials. Most common rotary tube furnaces are aligned horizontally, and depending on your laboratory needs and the manufacturer, they can be customized to be aligned at different angles or even vertically.

Across International - Compact Rotary Top-Open Tube Furnace

  • Atmosphere Laboratory Furnace

An atmosphere furnace provides the perfect environment for various procedures in many laboratories, providing the controlled temperature and specific mixture of gases specialized projects require. The term "atmosphere" denotes the controlled environment within the furnace that affects the chemical reactions during heating or processing. This atmosphere can be precisely tailored by adjusting the composition of the gases present. The controlled atmosphere is desired to complete tasks that require exact temperatures with no room for error. This is the best way to ensure the successful outcome of your project because it is sealed tightly to ensure the proper environment.

One of the main components of the atmosphere furnace is the correct mixture of gasses like hydrogen, nitrogen, or argon to create a specific chemical environment for the sample. These laboratory furnaces can heat materials up to 1700°C. 

The precise measurement of each gas is essential to the success of your project. You can use a separate chamber to mix the gases, which are then pumped into the furnace chamber where the work will be completed when they are done mixing. It is essential that the separate chamber that holds the gases does not receive any outside air because it could throw off the gas mixture and render your project useless.

Across International GCF1700 Controlled Atmosphere Muffle Furnace


In conclusion, each type has its own unique features and benefits that cater to different projects and experiments. It is crucial to understand your specific needs and choose the appropriate furnace accordingly. Let's dive into its applications and the factors to consider when purchasing a laboratory furnace in our next article.