Factors to consider when purchasing a muffle furnace.

By Miriam Carrillo, 17 October 2024

As muffle furnaces are available in different configurations, it is essential to consider what maximum temperature your application requires, chamber size, heating elements, and programming options. 

In this article, we will explore key factors to consider and the different uses for each type of laboratory furnace.

  • Temperature range
  • The primary point to consider is the required temperature.

    Muffle furnaces are available with a range of maximum temperatures. The time required for a muffle furnace to reach maximum temperature is dependent on a number of factors including the size of the furnace, the maximum power available, and the material used in the construction of the furnace. A small laboratory scale furnace with low thermal mass insulation can reach maximum temperature in as little as 20 minutes, whereas a larger scale furnace using dense refractory materials may take several hours to reach maximum temperature.

    Across International Muffle Furnaces size and temperature relation.1

    The most common have metallic wire heating elements with a maximum temperature in the range of 1000°C to 1200°C. Muffle furnaces with silicon carbide heating elements can achieve 1600°C and with molybdenum disilicide heating elements can achieve 1800°C.

    Across International Muffle Furnace models and specifications. 2

  • Chamber size
  • Based on your laboratory needs, be sure to select a muffle furnace with a chamber that is large enough to comfortably fit your samples. If it is too big, you will waste energy by heating more space than necessary.

  • Door opening style
  • Muffle furnaces come with various door types, usually front-loading, but they can open upwards, sideways, or downwards, each offering distinct benefits. The ideal choice for your lab depends on space constraints and your specific requirements. Sliding doors are suitable for compact spaces, whereas hinged doors allow easier access to the furnace's interior. If visibility into the furnace during operation is necessary, a windowed door might be the best option.

  • Programs and computer options
  • The simplest muffle furnaces enable users to set and monitor the temperature, making them ideal for labs that only need to cure materials without controlling heating time. However, for materials testing, a more advanced furnace with precise control over temperature ramp and time may be necessary.

    There are a few other important factors to keep in mind. Many basic furnaces can be upgraded with additional features. These could include a chimney or exhaust system to vent smoke or gasses from the chamber or to collect them for sampling. Other valuable upgrades might be ports for connecting extra monitoring equipment or allowing an air inlet, as well as additional timers, alarms, data loggers, USB ports for data downloads, and accessories like sample trays or stands.

    Types of muffle furnaces and its applications.

    When selecting the best furnace for your heat treatment requirements, the choice comes down to two leading options: tube furnaces and muffle furnaces. 

    Choosing the right furnace is essential for achieving optimal results and ensuring the purity and quality of your samples. Understanding the functions and applications of each type of furnace will guide you in selecting the best option for your needs. Let’s explore the different types of furnaces available on the market.

    • Box Laboratory Furnace

    A box furnace is a versatile piece of equipment used for high-temperature applications. Box furnaces use swing out doors or vertical lifts to allow products in a range of sizes to be put inside the furnace. Commonly used in chemistry, materials science, and engineering. These furnaces have a wide temperature range and can heat materials up to 1800°C.

    This type of laboratory furnace is used for heat-treating, calcining, pre-heating, tempering, and high-temperature processes

    • Muffle Laboratory Furnace

    Muffle furnaces are a subclass of box furnace: they are compact countertop heating sources with insulated fire brick walls to maintain high temperatures. This is ideal for ashing samples, heat treating applications, and materials research

    Muffle laboratory furnace can heat up to 1200°C and can handle a variety of materials like ceramics, glass, metals, and plastics.

    Across International Ai 1050 Compact Muffle Furnace

    • Tube Laboratory Furnace

    Tube furnaces come in various types, each tailored to meet a wide range of industrial needs and specifically designed for certain applications as purification, coating, drying, hardening, or aging of samples. A tube furnace can also be used for annealing, brazing, calcination, degassing, sintering, soldering, sublimation, synthesis, and tempering.

    Their main advantage against box furnaces is that tube furnaces are ideal for processing smaller samples due to their limited volume capacity and rapid heat up times. Additionally, they provide a controlled atmosphere around the samples, helping to preserve purity and prevent contamination.

    They are divided into 3 types, the rotary tube furnace which excels in continuous processing and powder heat treatment due to its rotating mechanism. Rotary tube furnaces are ideal for applications like powder metallurgy, material blending, and chemical reactions, where uniform heating and continuous mixing are vital. Their rotating mechanism ensures even temperature distribution and prevents the settling of samples, which is crucial for consistent processing and analysis. The rotation improves heat transfer efficiency, resulting in quicker processing times and more consistent outcomes.

    Compact Rotary Top-Open Tube Furnace

    The horizontal tube furnace provides uniform heating and easy access, making it ideal for research and small-scale production. Optimal for annealing, material testing and chemical processing, a horizontal tube furnace can be used in applications where samples need to be observed or rotated during processing. It is also suitable for applications where long, continuous tubes are required. The horizontal design of these tube furnaces facilitates easy sample placement and removal, making them perfect for experiments requiring manipulation or observation during heating. Their ability to provide uniform heating ensures consistent results, which is essential for research and quality control in laboratory settings.

    The vertical tube furnace, known for its design which is particularly useful for applications where space is a constraint or where the process benefits from a vertical setup. This type can also reach high temperatures and can be equipped with various types of heating elements, such as molybdenum disilicide or ceramic fiber elements. Its design is well-suited for processes where the sample needs to be introduced from the top and are typically used for applications that require uniform heating of a sample or material, such as calcination and it is a preferred option for high-temperature sintering.

    The vertical setup can aid in certain processes where gravity assists in the experiment or manufacturing process, ensuring even distribution of heat and materials.

    • Atmosphere Laboratory Furnace

    This vacuum atmosphere furnace is ideal for vacuum atmosphere brazing, sintering, surface treatment, thermal heat treatment and high temperature material process including stainless steel, titanium, aerospace material, silicon carbide wafer, other metals and ceramics. The controlled atmosphere is desired to complete tasks that require exact temperatures with no room for error. One of the main components of the atmosphere furnace is the correct mixture of gasses like hydrogen, nitrogen, or argon to create a specific chemical environment for the sample.  This is the best way to ensure the successful outcome of your project because it is sealed tightly to ensure the proper environment and they can heat materials up to 1700°C. 

    Across International GCF1700 Controlled Atmosphere Muffle Furnace

    Choosing the right muffle furnace is crucial for your laboratory's efficiency and success. By carefully evaluating these factors, you can ensure that your investment meets your specific needs and enhances your research capabilities. We hope this guide helps you make an informed decision and optimize your lab's performance.


    References: 

    1. https://ebioquim.com/wp-content/uploads/2019/04/Across_Full_Catalog_Updated-11.pdf
    2. https://www.labequip.com/stock/pictures/n1948.pdf